Principles Of Instrumental Analysis 6th Edition Ebook Download
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Sample questions asked in the 6th edition of Principles of Instrumental Analysis:
An operational amplifier has output voltage limits of +13V and -14 V when used with a ±15 V power supply. If the amplifier is used as a comparator, by what amount does ? + have to exceed ? - and? - have to exceed ? + for the amplifier to be at limit of the open-loop gain A is (a) 200,000 (b) 500,000 (c) 1.5 × 10 6
In a magnetic sector (single-focusing) mass spectrometer, it might be reasonable under some circumstances to monitor one mlz value, to then monitor a second m/z, and to repeat this pattern in a cyclic manner. Rapidly switching between two accelerating voltages while keeping all other conditions constant is called peak matching. (a) Derive a general expression that relates the rat io of the accelerating voltages to the ratio of the correspondi ng mlz values. (b) Use this equation to calculate mlz of an unknown peak if mlz of the ion used as a standard, CF 3 + , is 69.00 and the ratio of V unknown / V standard is 0.965035. ( c) Based on your answer in part (b ), and the assumption that the unknown is an organic compound that has a mass of 143, drnw some conclusions about your answer in part (b ), and about the compound.
(a) Calculate the standard potential for the reaction For CuBr, K sp = 5.2 X 10 -9 . (b) Give a schematic representation of a cell with a copper indicator electrode and a reference SCE that could be used for the determination of Br 2 . (c) Derive an equation that relates the measured potential of the cell in (b) to pBr (assume that the junction potential is zero). (d) Calculate the pBr of a bromide-containing solution that is saturated with CuBr and contained in the cell described in (b) if the resulting potential is - 0.095 V.
Principles of Instrumental Analysis, 5th Edition
Book Title :Principles of Instrumental Analysis, 5th Edition
This text is written for a course that deals with the principles and applications of modern analytical instruments. Emphasis is placed upon the theoretical basis of each type of instrument, its optimal area of application, its sensitivity, its precision, and its limitations. The text also introduces students to elementary integrated circuitry, microprocessors and computers, and treatment of analytical data.
Author(s) :Douglas A. Skoog; F. James Holler; Timothy A. Nieman (1997)
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